HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 846202Generated: October 30, 2026
N-bromobutanimide → HCID 19884897, compound
https://huagongshe.com/reaction/846202
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 19884952 | HCID 19884952 | — |
| Catalyst | Benzoyl Peroxide | HCID 7187 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 19884897 | HCID 19884897 | 100.4% |
Reaction Steps
A mixture of 26.2 g (0.1 mol) of 1-phenyl-3-(1-naphthalenyloxy)propane, 17.8 g (0.1 mol) of N-bromosuccinimide, 120 ml of carbon tetrachloride and 250 mg of benzoyl peroxide was heated at 80° C. for four hours. The mixture was cooled and the precipitated solid was collected by vacuum filtration. The mother liquor was concentrated under vacuum to provide 34.26 g of a red oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05135947 |
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| Source dataset | uspto-grants-1992_08 |
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| ORD ID | ord-5a4221342ca94ddf9850c2745e65b3a5 |
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| Source note | uspto-grants-1992_08 |
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