4-Methoxy-gamma-oxobenzenebutanoic acid → HCID 131717480, compound
Reaction equation
C[O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9](=[O:18])[CH2:10][C:11]([CH3:17])([CH3:16])[C:12]([O:14][CH3:15])=[O:13])=[CH:5][CH:4]=1.COC1C=CC(C(=O)CCC(O)=O)=CC=1>>[OH:2][C:3]1[CH:4]=[CH:5][C:6]([C:9](=[O:18])[CH2:10][C:11]([CH3:16])([CH3:17])[C:12]([O:14][CH3:15])=[O:13])=[CH:7][CH:8]=1Participants
3
Procedure
Following the procedure of Step B of Example 1 but substituting the product from Step B of this example for 4-methoxy-gamma-oxobenzenebutanoic acid there was obtained 4-hydroxy-alpha,alpha-dimethyl-gamma-oxobenzenebutanoic acid, methyl ester.
Sources & evidence
- ORD record
- ord-1346c3541ce0427d99933933cb6b01f6
- Source dataset
- uspto-grants-1992_08
- Patent number
- US05135940
Reaction notes
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