Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 16652-71-4 | HCID 3084256 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Proline benzyl ester | HCID 99767 | 96.3% |
Reaction Steps
A mixture of 3.18 g of benzyl DL -prolinate hydrochloride, 3 ml of demineralized water, 25 ml of benzene and 1.34 g of triethylamine was stirred at 20° C. for one hour and the decanted organic phase was washed with water, dried and evaporated to dryness to obtain 2.6 g of benzyl DL-prolinate in the form of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05136050 |
|---|
| Source dataset | uspto-grants-1992_08 |
|---|
| ORD ID | ord-336e74dcd40e4091b5b8a1744d1fc611 |
|---|
| Source note | uspto-grants-1992_08 |
|---|
