HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → D-Leucine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 67908467 | HCID 67908467 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | D-Leucine | HCID 439524 | — |
Reaction Steps
A mixture of 0.5 g of benzyl D-leucine hydrochloride, 20 ml of acetic acid and 20 ml of methanol was stirred with palladium under a hydrogen atmosphere until absorption ceased and the mixturewas filtered. The filtrate was evaporated to dryness under reduced pressure and the residue was chromatographed over silica gel to obtain D-leucine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05136050 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-b14c2de93bae49ffa22e4b4f29c7aeb5 |
| Source note | uspto-grants-1992_08 |