反应详情

To a solution of 1.82 g of the compound obtained in Example 1 dissolved in 50 ml of ethanol was added 500 mg of 5% palladium on charcoal. Catalytic reduction was carried out under atmospheric pressure for about 1 hour. The catalyst was removed by filtration, and the solvent was removed under reduced pressure to yield the titled compound. This product was used in the next step without further purification.

1. customThe catalyst was removed by filtration
2. customthe solvent was removed under reduced pressure