Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 54289634 | HCID 54289634 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131717481 | HCID 131717481 | — |
Reaction Steps
10 g (0.04 mole) of 2-(4-chlorobenzylidene)-5,5-dimethycyclohexanone prepared according to Example 1(a) were dissolved in 50 ml dichloromethane and cooled to 5-10° C. Bromine (6.4 g, 0.04 mole) was added over 5 minutes to give 2-bromo-2-(α-bromo-4-chlorobenzyl-5,5-dimethylcyclohexanone in solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05136081 |
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| Source dataset | uspto-grants-1992_08 |
|---|
| ORD ID | ord-099cc6f1067a484b8995422db853b1e4 |
|---|
| Source note | uspto-grants-1992_08 |
|---|
