Ethanol → HCID 19705038, compound

HRID 846401Notes

Reaction equation

HRID 846401 reaction equation
[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([C:9]2[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][C:10]=2[Cl:16])=[C:4]([C:17]([OH:19])=[O:18])[N:3]=1.S(=O)(=O)(O)O.[CH2:25](O)[CH3:26]>>[CH2:25]([O:18][C:17]([C:4]1[N:3]=[C:2]([NH2:1])[N:7]=[C:6]([NH2:8])[C:5]=1[C:9]1[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][C:10]=1[Cl:16])=[O:19])[CH3:26]

Participants

4

Reactant 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 19705121HCID 19705121, compound

Product 1

HCID 19705038HCID 19705038, compound

Procedure

This compound was prepared from the compound of Example 73 by refluxing in ethanol in the presence of concentrated sulphuric acid, mp. 177.5° C.

Sources & evidence

ORD record
ord-a8b5353bcac1484ea70afc26cb13fe54
Source dataset
uspto-grants-1992_08
Patent number
US05136080

Reaction notes

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