HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 3-Hydroxyacetanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-Hydroxyacetanilide | HCID 12124 | 89.3% |
Reaction Steps
In the manner of Example 2, Step A, the reaction of 66.0 g (0.60 mole) of 3-aminophenol and 77.8 g (0.76 mole) of acetic anhydride in 180 mL of water gave 81.0 g of 3-hydroxyacetanilide as a solid, mp 144°-146.C. The reaction was repeated to obtain an additional quantity of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05136868 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-d5a1865025ff494bbe3fa5fc2f10d366 |
| Source note | uspto-grants-1992_08 |