HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 4-Methyl-3-nitroanisole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Nitro-p-cresol | HCID 16271 | — |
| Product | 4-Methyl-3-nitroanisole | HCID 87137 | 97.5% |
Reaction Steps
In the manner of Example 8, Step C, the reaction of 25.0 g (0.162 mole) of 4-methyl-3-nitrophenol, 23.3 g (0.168 mole) of potassium carbonate, and 34.1 9 (0.24 mole) of methyl iodide produced 26.4 g of 1-methoxy-4-methyl-3-nitrobenzene as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05136868 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-f6464f96dad34604b0156565e6c576fd |
| Source note | uspto-grants-1992_08 |