HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 19883609, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | HCID 19883599 | HCID 19883599 | — |
| Product | HCID 19883609 | HCID 19883609 | 86% |
Reaction Steps
Using a similar procedure to that described in Example 4, (+)-2-[5-fluoro-3-(naphth-2-ylthio)phenyl]butane-1,2-diol was reacted with acetaldehyde. There was thus obtained as a 2:1 mixture of diastereoisomers (+)-4-ethyl-4-[5-fluoro-3-(naphth-2-ylthio)phenyl]-2-methyl-1,3-dioxolane in 86% yield as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137913 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-8befcfb860574c008b0db409f0899cd8 |
| Source note | uspto-grants-1992_08 |