HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Dimethoxy-pyrrolidine benzyl carbamate → 3,3-Dimethoxypyrrolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Dimethoxy-pyrrolidine benzyl carbamate | HCID 86746061 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3,3-Dimethoxypyrrolidine | HCID 11029882 | — |
Reaction Steps
The 2.21 g of 3,3-dimethoxy-pyrrolidine benzyl carbamate, from step 3, dissolved in 100 mL of methanol, 2.21 g of Pd/C (wet) was added, and placed under 4 atm of hydrogen for 20 hours. The catalyst was filtered off using a 0.45 micro millipore filter and the solvent was evaporated to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137892 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-8db8cb3449b64d54a778053f320dfcbb |
| Source note | uspto-grants-1992_08 |