HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67785161, compound → HCID 19883664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67785161 | HCID 67785161 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19883664 | HCID 19883664 | 98% |
Reaction Steps
1.12 g of 4-[(Z)-7-(dimethylamino)-1-heptenyl]benzophenone were dissolved in 30 ml of methanol, 20 mg of 5 percent palladium on carbon were added thereto and the suspension was stirred under hydrogen at normal pressure and room temperature for 2.5 hours. The reaction mixture was filtered through silica gel and the filtrate was evaporated. There were obtained 1.10 g (98%) of 4-[7-(dimethylamino)heptyl]benzophenone as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137920 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-0a5f69f9f57f428b8c3002107006fb42 |
| Source note | uspto-grants-1992_08 |