HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14054010, compound → N-(2-Aminophenyl)-4-(2-methylpropanamido)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14054010 | HCID 14054010 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-(2-Aminophenyl)-4-(2-methylpropanamido)benzamide | HCID 13961300 | — |
Reaction Steps
13.1 g (40 mMole) N-(2'-nitrophenyl)-4-isobutyrylaminobenzamide are hydrogenated under standard conditions in 400 mL tetrahydrofuran in the presence of 10% palladium charcoal. After concentrating the solvent to 120 mL, the precipitated crystals are filtered off with suction. Yield 10.2 g (86% of theory); m.p. 247.6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137918 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-91f942fbdb7b460cae859dad52e3de2f |
| Source note | uspto-grants-1992_08 |