Acetic Acid → HCID 86744314, compound

HRID 846873Notes

Reaction equation

HRID 846873 reaction equation
[F:1][C:2]1[C:13]([F:14])=[CH:12][C:5]([C:6]([CH2:8][C:9]([O-:11])=[O:10])=[O:7])=[C:4]([N+:15]([O-:17])=[O:16])[CH:3]=1.[CH2:18]([O:20][CH:21]([O-])[O-])[CH3:19].[C:24](O)(=O)[CH3:25]>>[F:1][C:2]1[C:13]([F:14])=[CH:12][C:5]([C:6]([C:8](=[CH:21][O:20][CH2:18][CH3:19])[C:9]([O:11][CH2:24][CH3:25])=[O:10])=[O:7])=[C:4]([N+:15]([O-:17])=[O:16])[CH:3]=1

Participants

4

Reactant 3

HCID 176Acetic AcidHCID 19884330HCID 19884330, compoundHCID 53630039Ethylorthoformate

Product 1

HCID 86744314HCID 86744314, compound

Procedure

To 3 ml of acetic acid anhydrous were added 3 g (0.01 mol) of ethyl (4,5-difluoro-2-nitrobenzoylacetate and 2.44 g (0.016 mol) of ethylorthoformate.

Sources & evidence

ORD record
ord-128018d0aea14e69acb3c74783e86bc4
Source dataset
uspto-grants-1992_08
Patent number
US05138088

Reaction notes

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