HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → L-Threonine methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | L-Threonine | HCID 6288 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | L-Threonine methyl ester | HCID 2734894 | — |
Reaction Steps
109 ml (1.5 mol) of thionyl chloride are added dropwise at 0° C. with strong cooling to 240 ml of methanol. 60 g (0.5 mol) of L-threonine are then added and the mixture is stirred at room temperature for 2 days, a clear solution resulting. After concentration, 85 g of a colorless oil are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05138091 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-70122c04209b4ef2a8790039f917ddeb |
| Source note | uspto-grants-1992_08 |