HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 44241894, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 57900153 | HCID 57900153 | — |
| Product | HCID 44241894 | HCID 44241894 | — |
Reaction Steps
Following the procedure of Example 15 and General Procedure C, 2-((2,4-difluorophenyl)(methyl)carbamoyl)-4H-thieno[3,2-c]chromene-8-carboxylic acid and dimethylamine were coupled to give 111bp. 1H NMR (400 MHz, CDCl3) δ 7.15-7.31 (m, 3 H), 6.82-7.00 (m, 4 H,), 5.13 (s, 2 H), 3.33 (m, 3 H), 2.94-3.13 (m, 6 H). LCMS (ESI) m/z: 429.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846762B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-9cb9db21798e49b79bd2cf677c3f9c0c |
| Source note | uspto-grants-2014_09 |