HCID 14835022, compound → 2-(3-Chloropropylsulfonylaminomethyl)-2-hexadecylthiomethyltetrahydrofuran

HRID 846974Notes

Reaction equation

HRID 846974 reaction equation
CO[CH:3](CSC(=O)NCCCCCCCCCCCCCCCCCC)[CH2:4]N.[Cl:29][CH2:30][CH2:31][CH2:32][S:33]([NH:36][CH2:37][CH:38]([O:57][CH3:58])[CH2:39][S:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][CH2:54][CH2:55][CH3:56])(=[O:35])=[O:34]>>[Cl:29][CH2:30][CH2:31][CH2:32][S:33]([NH:36][CH2:37][C:38]1([CH2:39][S:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH2:52][CH2:53][CH2:54][CH2:55][CH3:56])[CH2:4][CH2:3][CH2:58][O:57]1)(=[O:34])=[O:35]

Participants

3

Reactant 2

HCID 14835022HCID 14835022, compoundHCID 149922632-Methoxy-3-octadecylcarbamoylthiopropylamine

Product 1

HCID 148350352-(3-Chloropropylsulfonylaminomethyl)-2-hexadecylthiomethyltetrahydrofuran

Procedure

2-Aminomethyl-2-hexadecylthiomethyltetrahydrofuran IV b1 is allowed to react and worked by the same procedure as described in (4). m.p. 44.5° to 45.5° C. The summary of the experimental condition and the physical data of the product are listed in the Table 7.

Workup

  1. customto react

Sources & evidence

ORD record
ord-b96ba56518d84219910b147306e4f122
Source dataset
uspto-grants-1992_08
Patent number
US05138067

Reaction notes

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