1-Hexadecylthio-3-trityloxy-2-propanol → HCID 14835038, compound

HRID 846977Notes

Reaction equation

HRID 846977 reaction equation
NCC1(CO[C:10](=[O:30])[NH:11][CH2:12]CCCCCCCCCCCCCCCCC)CCCO1.[CH2:31]([S:47][CH2:48][CH:49]([OH:71])[CH2:50]OC(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1)[CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH3:46].[Cl:72][CH2:73][CH2:74][CH2:75][S:76]([NH:79]CC(OC)CSCCCCCCCCCCCCCCCC)(=[O:78])=[O:77]>>[Cl:72][CH2:73][CH2:74][CH2:75][S:76]([NH:79][CH2:50][CH:49]([O:71][C:10](=[O:30])[NH:11][CH3:12])[CH2:48][S:47][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH3:46])(=[O:78])=[O:77]

Participants

4

Reactant 3

HCID 130028641-Hexadecylthio-3-trityloxy-2-propanolHCID 14834997HCID 14834997, compoundHCID 14835022HCID 14835022, compound

Product 1

HCID 14835038HCID 14835038, compound

Procedure

3-Hexadecylthio-2-methylcarbamoyloxypropylamine IV c1 is allowed to react and worked up by the same procedure as described in (4). m.p. 84.5°-85.5° C. The summary of the experimental condition and the physical data of the product are listed in the Table 7.

Workup

  1. customto react

Sources & evidence

ORD record
ord-934ecbabc40f4a8a8f697e9f7bfc4931
Source dataset
uspto-grants-1992_08
Patent number
US05138067

Reaction notes

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