HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diaminomaleonitrile → 2-butyl-1H-imidazole-4,5-dicarbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diaminomaleonitrile | HCID 2723951 | — |
| Reactant | Ethyl pentanimidate hydrochloride | HCID 12283341 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-butyl-1H-imidazole-4,5-dicarbonitrile | HCID 5260591 | — |
Reaction Steps
Ethyl pentanimidate hydrochloride (42.66 g, 257.8 mmol, 1 eq), diaminomaleonitrile (27.90 g, 258.1 mmol, 1 eq) and pyridine (400 mL) were mixed and refluxed for 48 hours under N2. The solvent was removed by rotary evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05138069 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-96638966e0cd47e08f991f481b488f95 |
| Source note | uspto-grants-1992_08 |