HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 15029853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 15029852 | HCID 15029852 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15029853 | HCID 15029853 | — |
Reaction Steps
The product of Example 60 was added to methyl ethyl ketone (50 ml), K2CO3 (5 g) and methyl iodide (5 ml) then heated at reflux for 41/2 hrs. The reaction was cooled, H2O added, followed by an EtOAc extraction. The organic layer was separated, washed with brine, dried (Na2SO4), filtered and evaporated. Trituration of the residue afforded the desired compound after filtration, m.p. 129°-30° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05140040 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-6e50e5c88bc744a499393045123b84fe |
| Source note | uspto-grants-1992_08 |