HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54031579, compound → HCID 15106480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54031579 | HCID 54031579 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15106480 | HCID 15106480 | 79.6% |
Reaction Steps
To a solution of 250 mg of ethyl o-[p-(3-phenoxypropoxy)benzamido]cinnamate obtained in Example 34 in 10 ml of methanol and 20 ml of ethyl acetate was added 10% palladium-carbon. Catalytic reduction was performed until absorption of hydrogen was discontinued. The catalyst was filtered off and the residue was recrystallized from isopropyl alcohol to obtain 200 mg of ethyl 3-[o-[p-(3-phenoxypropoxy)benzamido]phenyl]propionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05140046 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-d33b6b55d0fa4e34bdf8958e857a2ce0 |
| Source note | uspto-grants-1992_08 |