HCID 15023212, compound → HCID 15023213, compound
Reaction equation
[Cl:1][C:2]1[CH:24]=[C:23]([C:25]([F:28])([F:27])[F:26])[CH:22]=[CH:21][C:3]=1[O:4][C:5]1[CH:17]=[CH:16][C:8]([O:9][CH:10]([CH3:15])[C:11](OC)=[O:12])=[C:7]([N+:18]([O-])=O)[CH:6]=1.ClC1C(OC2C=CC3OC(C)C(=O)NC=3C=2)=NC=C(C(F)(F)F)C=1>>[Cl:1][C:2]1[CH:24]=[C:23]([C:25]([F:28])([F:27])[F:26])[CH:22]=[CH:21][C:3]=1[O:4][C:5]1[CH:17]=[CH:16][C:8]2[O:9][CH:10]([CH3:15])[C:11](=[O:12])[NH:18][C:7]=2[CH:6]=1Participants
3
Procedure
In Example 1, methyl 2-[4-(2-chloro-4-trifluoromethylphenoxy)-2-nitrophenoxy]propionate was used instead of methyl 2-[5-(2-chloro-4-trifluoromethylphenoxy)-2-nitrophenoxy]propionate to prepare the title compound, and 6-(3-Chloro-5-trifluoromethyl-2-pyridyloxy)-2-methyl-2H-1,4-benzoxazine-3 (4H)-one (Example 16) was prepared in the same manner as described above.
Sources & evidence
- ORD record
- ord-2e23e03178944909962b78171968515f
- Source dataset
- uspto-grants-1992_08
- Patent number
- US05141551
Reaction notes
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