Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Melamine | HCID 7955 | — |
| Solvent | Water | HCID 962 | — |
| Product | Melamine formaldehyde | HCID 93374 | — |
Reaction Steps
To 385 g of a distilled water were added 71.3 g of melamine and 118 g of formalin, and the resulting mixture was heated at 60° C. for 30 minutes under stirring to obtain a melamine-formalin precondensate. 77.1 g of the melamine-formalin precondensate was added to the above-obtained dispersion (Dispersion I), and the resulting mixture was again adjusted to pH 6.0 using a 20 % aqueous solution of phosphoric acid. The mixture was then heated at 60° C. for 90 minutes under stirring, to prepare a dispersion of microcapsules (Microcapsule-dispersion J), each microcapsule having a melamine-formaldehyde resin wall.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05141679 |
|---|
| Source dataset | uspto-grants-1992_08 |
|---|
| ORD ID | ord-f91ee290c6e84c3883beb4b5bb5ef7bc |
|---|
| Source note | uspto-grants-1992_08 |
|---|