HCID 15713246, compound → HCID 15713247, compound

HRID 847376Notes

Reaction equation

HRID 847376 reaction equation
[CH:1]([N:3]1[CH:8]([C:9]([O:11]CC)=[O:10])[CH2:7][C:6](=[CH2:14])[CH2:5][CH:4]1[C:15]([O:17]CC)=[O:16])=[O:2]>C1CCCCC1.C(OCC)(=O)C>[CH:1]([N:3]1[CH:8]([C:9]([OH:11])=[O:10])[CH2:7][C:6](=[CH2:14])[CH2:5][CH:4]1[C:15]([OH:17])=[O:16])=[O:2]

Participants

3

Reactant 1

HCID 15713246HCID 15713246, compound

Product 1

HCID 15713247HCID 15713247, compoundYield 51.2%

Reagents, catalysts & solvents 1

HCID 21867204Cyclohexane ethylacetateSolvent

Procedure

Using the procedure of Step D of Example 1, 997 mg of the product of Step C were reacted to obtain 404 mg of the desired product with a Rf=0.2, eluant ethanol-ammonium hydroxide (8-2).

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-0107abaaa81b4d24ba1d61157c9b3df3
Source dataset
uspto-grants-1992_08
Patent number
US05141952

Reaction notes

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