HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[(dimethylamino)methyl]benzonitrile → HCID 19881402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[(dimethylamino)methyl]benzonitrile | HCID 826329 | — |
| Reactant | Phosphonium | HCID 5460504 | — |
| Reactant | Arsonium | HCID 5460506 | — |
| Reactant | HCID 19881404 | HCID 19881404 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19881402 | HCID 19881402 | — |
Reaction Steps
A mixture of (B) and N,N-dimethyl-4-cyano benzylamine in acetonitrile was refluxed for 2 hours. The reaction mixture was then poured into diethyl ether, and the crude product was collected by filtration. The crude product was recrystallized from ethanol. The same reaction can be used to prepare the corresponding phosphonium and arsonium salts.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05141969 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-c99f46cb7eb8477eb0e8a2917d7c6568 |
| Source note | uspto-grants-1992_08 |