HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Naphthoquinone → HCID 15657226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Naphthoquinone | HCID 8530 | — |
| Reactant | Benzenesulfinic acid, sodium salt | HCID 2723840 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15657226 | HCID 15657226 | — |
Reaction Steps
1,4-naphthoquinone (15.8 g) was dissolved in 100 ml of a mixture of ethyl acetate and acetic acid (9:1) and sodium benzenesulfinate (24.6 g) was added. The resulting mixture was stirred for 5 hours and the obtained crystals were filtered and washed with a small amount of acetone. (Yield: 22.5 g)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142029 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-cbf518ddd34040faaa87d5c0578915c2 |
| Source note | uspto-grants-1992_08 |