HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 847464Generated: October 30, 2026
3,4-Dichloroaniline → HCID 19006436, compound
https://huagongshe.com/reaction/847464
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3,4-Dichloroaniline | HCID 7257 | — |
| Reactant | HCID 19006427 | HCID 19006427 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19006436 | HCID 19006436 | — |
Reaction Steps
26.0 g of 2-(2,6-dichlorophenyl)-thiazoline-4,5-dione are suspended in 250 ml of dry toluene and heated to 90° C. while stirring. Gas is evolved and a violet solution is obtained, to which is added 16.2 g of 3,4-dichloroaniline dissolved in 30 ml of toluene. After stirring for 15 minutes the solution is cooled and the precipitate obtained is drawn off. Yield 20.1 g. Melting point 168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05142064 |
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| Source dataset | uspto-grants-1992_08 |
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| ORD ID | ord-14d3ec7d7f5040c1994ec0bf47ee69e8 |
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| Source note | uspto-grants-1992_08 |
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