HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → Silane, (2,2-dimethylpropoxy)trimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Neopentyl alcohol | HCID 6404 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Product | Silane, (2,2-dimethylpropoxy)trimethyl- | HCID 552401 | — |
Reaction Steps
1 mole of neopentyl alcohol and 1.5 moles of trimethylchlorosilane together with 0.0005 moles of tetra-n-butyl ammonium bromide were heated under reflux (54°-100° C.) until the IR spectrum did not show an OH band. The product was worked up by fractional distillation at normal pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142081 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-8de40803379b411cadce39897c066ac6 |
| Source note | uspto-grants-1992_08 |