HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butanol → tert-Butoxytrimethylsilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butanol | HCID 6386 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Product | tert-Butoxytrimethylsilane | HCID 554467 | — |
Reaction Steps
1 mole of tert. butanol, 1.5 moles of trimethylchlorosilane and 0.001 moles of tetra-n-butyl ammonium bromide were reacted at the reflux temperature (54°-67° C.) as in Example 1 and then worked up by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142081 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-5185b9c01b934976bac5718144134241 |
| Source note | uspto-grants-1992_08 |