HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → 3,8-Dioxa-2,9-disiladecane, 2,2,9,9-tetramethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | 1,4-Butanediol | HCID 8064 | — |
| Catalyst | Hexadecyltributylphosphonium bromide | HCID 84716 | — |
| Product | 3,8-Dioxa-2,9-disiladecane, 2,2,9,9-tetramethyl- | HCID 140321 | — |
Reaction Steps
1 mole of butane-1,4-diol, 3 moles of trimethylchlorosilane and 0.002 moles of tributyl-hexadecyl phosphonium bromide were reacted at the reflux temperature (56°-96° C.) as in Example 1. The product was worked up by fractional distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142081 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-9db4bfcea3d94061a42271e73442d436 |
| Source note | uspto-grants-1992_08 |