HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → Butoxy(triethyl)silane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Chlorotriethylsilane | HCID 13819 | — |
| Catalyst | Benzyl triethylammonium chloride | HCID 66133 | — |
| Solvent | P-Xylene | HCID 7809 | — |
| Product | Butoxy(triethyl)silane | HCID 525735 | — |
Reaction Steps
0.1 moles of n-butanol, 0.15 moles of triethylchlorosilane and 0.0005 moles of triethylbenzyl ammonium chloride in 50 ml of p-xylene were heated under reflux (80°-110° C.). When the evolution of HCl had ceased, the product was worked up by fractional distillation at reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142081 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-adda96e4f7b048839a4c5ba7b0701f31 |
| Source note | uspto-grants-1992_08 |