(Diethylamino)sulfur trifluoride → HCID 22910044, compound

HRID 847589Notes

Reaction equation

HRID 847589 reaction equation
[C:1]1([CH2:7][CH2:8][S:9]([CH2:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(N(S(F)(F)[F:25])CC)C>ClCCl>[C:1]1([CH2:7][CH2:8][S:9][CH:11]([F:25])[CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 123472(Diethylamino)sulfur trifluorideHCID 12548238HCID 12548238, compound

Product 1

HCID 22910044HCID 22910044, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

According to the procedure of McCarthy et. al. (J. Amer. Chem. Soc. 1985, 107, 735), the resultant compound of Example 2 was treated with diethylaminosulfur trifluoride in dichloromethane to give the desired compound.

Sources & evidence

ORD record
ord-693b4837a0ec4835adb0686e8693da75
Source dataset
uspto-grants-1992_08
Patent number
US05142056

Reaction notes

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