Borane → 1,5-Diphenylpentan-3-amine

HRID 847590Notes

Reaction equation

HRID 847590 reaction equation
[C:1]1([CH2:7][CH2:8][C:9](=[N:18]O)[CH2:10][CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.B>>[NH2:18][CH:9]([CH2:10][CH2:11][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1)[CH2:8][CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 6331BoraneHCID 225565N-(1,5-diphenylpentan-3-ylidene)hydroxylamine

Product 1

HCID 153888741,5-Diphenylpentan-3-amine

Procedure

According to the procedure of Feuer and Braunstein (J. Org. Chem. 1969, 34, 1817), the resultant compound of Example 31 was treated with borane to give the desired compound.

Sources & evidence

ORD record
ord-cb39e663455d45d8aa0fa4d5c80f6a13
Source dataset
uspto-grants-1992_08
Patent number
US05142056

Reaction notes

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