HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 22910217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | ((2-Hydroxy-3-(phenylsulfanyl)propyl)sulfanyl)benzene | HCID 12671306 | — |
| Reactant | 1,5-Diphenylpentan-3-ol | HCID 12838510 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 22910217 | HCID 22910217 | — |
Reaction Steps
Using the procedure of Example 51 but 1,5-diphenyl-3-pentanol with the resultant compound of Example 15 gave, after silica gel chromatography using 15% ethyl acetate in hexane, 44 mg (31%) of the desired compound (Rf 0.27, 20% ethyl acetate in hexane). 1H NMR (CDCl3) δ 3.21 (dd, J=15, 6 Hz, 2H), 3.26 (dd, J=15, 6 Hz, 2H), 3.40 (s, 3H), 3.91 (pentet, J=6 Hz, 1H), 4.68 (s, 2H), 7.15-7.35 (m, 10H). Mass spectrum (M +NH4)+ =338.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05142056 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-cf5c922ede6d4de0b2e5d23340c39d52 |
| Source note | uspto-grants-1992_08 |