HuagongsheHuagongshe Chemistry Print Report · For research reference only
Terephthaloyl chloride → HCID 86738026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Terephthaloyl chloride | HCID 7488 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 20566781 | HCID 20566781 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 86738026 | HCID 86738026 | — |
Reaction Steps
Terephthaloyl chloride (6.1 g, 0.03 mole) in 30 ml benzene was added dropwise to a mixture of dicyclohexyl hydroxymethyl phosphine oxide and triethylamine at 50° C. maximum. The reaction mixture was heated to reflux for 30 minutes and the product was filtered, washed with water and dried; m.p. 226°-228.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04293465 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-196202f8ac1d47b6a9a8d7955064d286 |
| Source note | uspto-grants-1981_10 |