2-Chlorobenzoyl isocyanate → L 7063

HRID 847714Notes

Reaction equation

HRID 847714 reaction equation
[Cl:1][C:2]1[CH:27]=[CH:26][CH:25]=[CH:24][C:3]=1[C:4]([NH:6][C:7]([NH:9][C:10]1[CH:15]=[N:14][C:13]([C:16]2[CH:21]=[CH:20][C:19]([Br:22])=[CH:18][CH:17]=2)=[C:12](Cl)[N:11]=1)=[O:8])=[O:5].N[C:29]1C=NC(C2C=CC(Br)=CC=2)=C(Cl)N=1.ClC1C=CC=CC=1C(N=C=O)=O>>[Cl:1][C:2]1[CH:27]=[CH:26][CH:25]=[CH:24][C:3]=1[C:4]([NH:6][C:7]([NH:9][C:10]1[CH:15]=[N:14][C:13]([C:16]2[CH:21]=[CH:20][C:19]([Br:22])=[CH:18][CH:17]=2)=[C:12]([CH3:29])[N:11]=1)=[O:8])=[O:5]

Participants

4

Reactant 3

HCID 99423112-Chlorobenzoyl isocyanateHCID 13341092HCID 13341092, compoundHCID 13341120HCID 13341120, compound

Product 1

HCID 155223L 7063

Procedure

1-(2-Chlorobenzoyl)-3-[5-(4-bromophenyl)-6-chloro-2-pyrazinyl]urea, weighing 1.4 g., and having a melting point of about 240°-242° C., from 0.9 g. of 2-amino-5-(4-bromophenyl)-6-chloropyrazine and 0.65 g. of 2-chlorobenzoylisocyanate.

Sources & evidence

ORD record
ord-b3c7948fad1e4717b8fc9e907d78d9f5
Source dataset
uspto-grants-1981_10
Patent number
US04293552

Reaction notes

Loading…