Dimethylcarbamoyl Chloride → HCID 12791208, compound

Participants

Reaction Steps

Following the procedure of Example 1C using 18.2 g. (0.1065 moles) of N,N-dimethyl-N'-(2-thiazolyl)-1,2-ethane diamine, 12.1 g. (0.120 moles) of triethylamine, 12.5 g. (0.116 moles) of dimethylcarbamoyl chloride and 135 ml. of dry benzene, there is obtained 20.1 g. of N,N-dimethyl-N'-(2-dimethylaminoethyl)-N'-(2-thiazolyl)urea as an oil which is distilled at 108°-110° C., at 0.02 mm. of Hg.

Provenance & Evidence