Methyl Isocyanate → HCID 178485936, compound

HRID 847853Notes

Reaction equation

HRID 847853 reaction equation
[NH:1]1[CH:5]=[CH:4][C:3]([CH2:6][NH:7][CH2:8][CH2:9][NH2:10])=[N:2]1.[CH3:11][N:12]=[C:13]=[O:14]>>[CH3:11][NH:12][C:13]([NH:10][CH2:9][CH2:8][NH:7][CH2:6][C:3]1[CH:4]=[CH:5][NH:1][N:2]=1)=[O:14]

Participants

3

Reactant 2

HCID 12228Methyl IsocyanateHCID 178511340HCID 178511340, compound

Product 1

HCID 178485936HCID 178485936, compound

Procedure

N-(3-Pyrazolylmethyl)ethylenediamine is reacted with methyl isocyanate by the procedure of Example 24 to give, after concentrating and separating the residue by column chromatography, the title compound.

Workup

  1. customto give
  2. concentrationafter concentrating
  3. customseparating the residue by column chromatography

Sources & evidence

ORD record
ord-1ded83a1700e454f9f56fca1e5896fb1
Source dataset
uspto-grants-1981_10
Patent number
US04293697

Reaction notes

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