(2-Isothiocyanatoethyl)dimethylamine → HCID 20557633, compound

HRID 847901Notes

Reaction equation

HRID 847901 reaction equation
[S:1]1[CH:5]=[CH:4][N:3]=[C:2]1[CH2:6][NH:7][CH2:8][CH2:9][NH2:10].[CH3:11][N:12]([CH3:18])[CH2:13][CH2:14][N:15]=[C:16]=[S:17]>>[CH3:11][N:12]([CH3:18])[CH2:13][CH2:14][NH:15][C:16]([NH:10][CH2:9][CH2:8][NH:7][CH2:6][C:2]1[S:1][CH:5]=[CH:4][N:3]=1)=[S:17]

Participants

3

Reactant 2

HCID 3853726(2-Isothiocyanatoethyl)dimethylamineHCID 17944882N-(2-thiazolylmethyl)ethylenediamine

Product 1

HCID 20557633HCID 20557633, compound

Procedure

Treating N-(2-thiazolylmethyl)ethylenediamine with 2-dimethylaminoethyl isothiocyanate by the procedure of Example 40, then concentrating and separating by column chromatography gives the title compound.

Workup

  1. concentrationconcentrating
  2. customseparating by column chromatography

Sources & evidence

ORD record
ord-6b5813aca1374676a7c462d4191470e1
Source dataset
uspto-grants-1981_10
Patent number
US04293697

Reaction notes

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