HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Phenylthio)thiophene → HCID 88771909, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Phenylthio)thiophene | HCID 2778902 | — |
| Reactant | O-(2,4,6-Trimethylbenzenesulfonyl)hydroxylamine | HCID 11830845 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 88771909 | HCID 88771909 | 65% |
Reaction Steps
In a manner analogous to that described in Example 1, Stage 1, from phenyl-(3-thienyl)-sulphide and O-mesitylsulphonyl-hydroxylamine in dichloromethane, there is obtained phenyl-(3-thienyl)-sulphimide mesitylene-sulphonate in a yield of 65% in theory; after recrystallisation from isopropanol, the compound melts at 116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294838 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-c67bc925bfc2499bbb4d3ebde7b8540a |
| Source note | uspto-grants-1981_10 |