HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylaminoethyl chloride → Sulfoximine, N-(2-(diethylamino)ethyl)-S-phenyl-S-3-pyridinyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylaminoethyl chloride | HCID 13364 | — |
| Reactant | S-phenyl-S-(3-pyridyl)-sulphoximide | HCID 20566260 | — |
| Product | Sulfoximine, N-(2-(diethylamino)ethyl)-S-phenyl-S-3-pyridinyl- | HCID 3054388 | 46% |
Reaction Steps
In a manner analogous to that described in Example 1, Stage 3, from S-phenyl-S-(3-pyridyl)-sulphoximide and 2-diethylaminoethyl chloride, there is obtained, in a yield of 46% of theory, N-(2-diethylaminoethyl)-S-phenyl-S-(3-pyridyl)-sulphoximide. The corresponding dibenzoyltartrate, after recrystallisation from isoporopanol, melts at 130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294838 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-138292bf2ba0430790baa1511fb8de5c |
| Source note | uspto-grants-1981_10 |