HRID848110

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID141233

Disodium

Na2

HCID350015

2-Chloro-6-ethoxy-1,3-benzothiazole

C9H8ClNOS

HCID15910000

α-Mercapto-α-methylbenzeneacetic acid

C9H10O2S

PRODUCTS

生成物

结构：CCOc1ccc2nc(SC(C)(C(=O)O)c3ccccc3)sc2c1

HCID174749

2-[(6-Ethoxy-1,3-benzothiazol-2-yl)sulfanyl]-2-phenylpropanoic acid

C18H17NO3S2

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID263

1-Butanol

C4H10O

PROCEDURE

实验过程

A mixture of 21.4 g of 2-chloro-6-ethoxybenzothiazole, 22.6 g of the disodium salt of 2-mercapto-2-phenylpropionic acid and 200 ml of n-butanol is boiled for 4 hours and is evaporated and worked up in the customary manner to give 2-(6-ethoxybenzothiazol-2-ylthio)-2-phenylpropionic acid, m.p. 152°-153°.

WORKUP

后处理

customis evaporated