HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromothiophenol → HCID 20566315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromothiophenol | HCID 66049 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 1,2,4-Oxadiazole, 3,5-bis(chloromethyl)- | HCID 6451206 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20566315 | HCID 20566315 | — |
Reaction Steps
4-Bromobenzenethiol (3.78 g, 0.02 mol) was added to a solution of sodium (0.46 g, 0.02 mol) in ethanol (50 ml.) and 3,5-di-(chloromethyl)-1,2,4-oxadiazole (1.67 g, 0.01 mol) was added dropwise. The solution was then filtered and evaporated to give a solid which was recrystallised from isopropanol to give 3,5-di-(4-bromophenylthiomethyl)-1,2,4-oxadiazole, m.p. 80°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294842 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-556bc0e14ebc447da967ec4af9df9acf |
| Source note | uspto-grants-1981_10 |