HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl chloroformate → HCID 20566336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl chloroformate | HCID 10387 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzenamine, 2-((1,2,4-oxadiazol-3-ylmethyl)thio)- | HCID 3057622 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20566336 | HCID 20566336 | — |
Reaction Steps
A solution of benzylchloroformate (3.79 g) and 3-(2-aminophenylthiomethyl)-1,2,4-oxadiazole (3.1 g) in dioxan (75 ml) containing potassium carbonate (3.15 g) was refluxed for 1 hour. Solvent was then removed by evaporation under reduced pressure to give a colourless solid which was re-crystallised from hexane to give 3-(2-benzyloxycarbonylaminophenylthiomethyl)-1,2,4-oxadiazole, m.p. 41°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294843 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-44be2cb32f404a8c93de1ca7462d8589 |
| Source note | uspto-grants-1981_10 |