HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → HCID 20566337, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Benzenamine, 2-((1,2,4-oxadiazol-3-ylmethyl)thio)- | HCID 3057622 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20566337 | HCID 20566337 | — |
Reaction Steps
A mixture of 3-(2-aminophenylthiomethyl)1,2,4-oxadiazole (4.14 g), 4-chlorobenzoyl chloride (3.68 g), sodium hydroxide (0.8 g) and water (15 ml) was stirred at 25° for 4 hours. Crude product was recovered by filtration and crystallised from ethanol to give 3-[2-(4-chlorobenzamido)phenylthiomethyl]-1,2,4-oxadiazole, m.p. 103°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294843 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-f61fb53e20f44433a9af42aa9ac33463 |
| Source note | uspto-grants-1981_10 |