HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrobenzenesulfenyl chloride → HCID 20566344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrobenzenesulfenyl chloride | HCID 24319 | — |
| Reactant | Benzenamine, 2-((1,2,4-oxadiazol-3-ylmethyl)thio)- | HCID 3057622 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20566344 | HCID 20566344 | — |
Reaction Steps
A solution of 2-nitrophenylsulphenyl chloride (1.44 g, 7.5×10-3 mol) in chloroform was added dropwise to a solution of 3-(2-aminophenylthiomethyl)-1,2,4-oxadiazole in chloroform (20 ml). The yellow mixture was stirred overnight, the crude product collected by filtration and recrystallised from ethyl acetate/hexane to give 3-[2-(2-nitrophenylsulphenylamino)phenyl]thiomethyl-1,2,4-oxadiazole, m.p. 90° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294843 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-15789ebc592e4c2d80ba5f0b59b3b428 |
| Source note | uspto-grants-1981_10 |