HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 20566448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | HCID 14150246 | HCID 14150246 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20566448 | HCID 20566448 | 71.3% |
Reaction Steps
51 g of 2-[4-(3-aminobenzamido)phenyl]-1-formylhydrazine and 29 g of calcium carbonate were dispersed in a mixture of 120 ml of dioxane and 120 ml of water. To the dispersion, 25 g of thiophosgene was added under cooling with ice. After reacting under cooling with ice for 3 hours, the crystals deposited were collected by filtration to obtain 42 g of the object compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294919 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-b7b1c3330d9943a89384b0a504dd24f4 |
| Source note | uspto-grants-1981_10 |