HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl fluoride, 4-(trifluoromethoxy)- → 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl fluoride, 4-(trifluoromethoxy)- | HCID 67612 | — |
| Reactant | 1,8-Diaminonaphthalene | HCID 68067 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE | HCID 12945439 | — |
Reaction Steps
1,8-Diaminonaphthalene (1.52 grams; 0.0096 mole) was dissolved in 25 ml. of toluene, then decanted. p-Trifluoromethoxybenzoyl fluoride (2.0 grams; 0.0096 mole) was dissolved in 25 ml. of toluene. Both solutions were added simultaneously to 25 ml. of toluene. After the reaction mixture had been stirred for approximately 4 hours, TLC indicated that the reaction was complete.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294964 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-05d553fa216b4f15b99e90ae303a1f63 |
| Source note | uspto-grants-1981_10 |