HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → Ethyl 4-chloro-2-[(hexyloxy)imino]-3-oxobutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | Ethyl 2-[(hexyloxy)imino]-3-oxobutanoate | HCID 53879425 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Ethyl 4-chloro-2-[(hexyloxy)imino]-3-oxobutanoate | HCID 54042766 | 80.2% |
Reaction Steps
Ethyl 2-n-hexyloxyimino-3-oxobutyrate (syn isomer, 60.7 g.), acetic acid (61 ml.) and sulfuryl chloride (34.7 g.) were treated in a similar manner to that of Example F-(2) to give ethyl 2-n-hexyloxyimino-4-chloro-3-oxobutyrate (syn isomer, 55.6 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294960 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-7558a9c526f149efa1a78b0b2b12d61d |
| Source note | uspto-grants-1981_10 |