HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromooctane → HCID 54485478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromooctane | HCID 8140 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178472877 | HCID 178472877 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54485478 | HCID 54485478 | 97.3% |
Reaction Steps
Ethyl 2-hydroxyimino-3-oxobutyrate (syn isomer, 100 g.), N,N-dimethylformamide (300 ml.), potassium carbonate (130 g.) and bromooctane (121 g.) were treated in a similar manner to that of Example F-(1) to give ethyl 2-n-octyloxyimino-3-oxobutyrate (syn isomer, 165.5 g.), oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04294960 |
| Source dataset | uspto-grants-1981_10 |
| ORD ID | ord-b57cad909c484eab9ababe1f581630c3 |
| Source note | uspto-grants-1981_10 |